Formation evaluation







Formation evaluation is a critical process in the oil and gas industry that involves analyzing the properties of rocks and fluids in a subsurface reservoir to determine their potential for producing hydrocarbons. This information is essential for making informed decisions about the viability of drilling and completing a well and optimizing production.

The process of formation evaluation typically involves collecting data from various sources, such as drill cuttings, wireline logs, and core samples. The data is then analyzed to determine the properties of the reservoir, such as its lithology, porosity, permeability, fluid content, and pressure.

Wireline logging is one of the most common techniques used for formation evaluation. It involves lowering a tool string, containing various sensors and detectors, into the wellbore to measure and record the physical properties of the rocks and fluids in the formation. Some of the measurements that can be taken with wireline logging include gamma ray, resistivity, neutron porosity, and sonic velocity.

Another technique that is often used in formation evaluation is core analysis. This involves taking samples of the rock formation from the wellbore and analyzing them in a laboratory to determine their physical and chemical properties. This information can be used to confirm and supplement the data obtained from wireline logging.

Overall, formation evaluation plays a crucial role in the oil and gas industry by providing critical information about the properties of subsurface reservoirs. This information is used to optimize production and maximize the recovery of hydrocarbons.

Applications :

  • Well Log analysis:

Well log analysis is the process of interpreting data obtained from well logs to evaluate the subsurface geology and formation properties of a well. Well logs are measurements of various properties of the rock formations and fluids penetrated by the well, which are recorded using sensors and instruments on a wireline cable.

Some common types of well logs include:

1.  Gamma ray logs: These logs measure the natural gamma radiation emitted by the rocks, which can help identify different rock types and determine the depth and thickness of individual formations.

2. Resistivity logs: These logs measure the electrical resistivity of the rocks, which can help identify the presence of hydrocarbons or water-bearing formations and estimate their properties.

3. Sonic logs: These logs measure the velocity of sound waves in the rocks, which can help determine the porosity and permeability of the rocks.

4. Density logs: These logs measure the density of the rocks, which can help estimate their lithology and porosity.

5. Neutron logs: These logs measure the neutron count rate in the rocks, which can help estimate their porosity and fluid content.

By analyzing the data obtained from well logs, geoscientists and engineers can build a subsurface model of the well, which can be used to optimize drilling and completion operations, plan production strategies, and evaluate the economic potential of the well.

Well log analysis can be a complex and challenging task, requiring expertise in geology, petrophysics, and reservoir engineering. However, with the help of advanced software tools and machine learning algorithms, well log analysis can be done more efficiently and accurately than ever before.

  • Petrophysical evaluation:
Petrophysical evaluation of rock samples typically involves measuring various physical and chemical properties of the rock in order to characterize its potential for containing hydrocarbons. Some common petrophysical properties that are typically measured include:

1. Porosity: the percentage of the rock's volume that is made up of pore spaces or voids. This property is important because it helps to determine how much oil or gas a rock can hold.
2. Permeability: the measure of the ability of the rock to allow fluids to flow through it. This property is important because it affects the flow of oil or gas through the rock.
3. Saturation: the percentage of the pore space that is filled with oil or gas. This property is important because it helps to determine the potential volume of hydrocarbons that can be extracted from the rock.
4. Density: the measure of the mass per unit volume of the rock. This property is important because it helps to determine the rock's mineralogy and lithology.
5. P-wave velocity: the speed at which seismic waves travel through the rock. This property is important because it can be used to estimate the rock's porosity, permeability, and fluid saturation.
6. Resistivity: the measure of the rock's ability to resist the flow of electric current. This property is important because it can be used to identify the presence of hydrocarbons in the rock.
7. Thermal conductivity: the measure of the rock's ability to conduct heat. This property is important because it can be used to estimate the rock's porosity and fluid saturation.
8. Rock mechanics: the measure of the rock's strength, elasticity, and deformation behavior. These properties are important because they affect the drilling and completion of the well, as well as the stability of the reservoir.
9. Grain size and shape: the size and shape of the individual mineral grains that make up the rock. This property is important because it can affect the rock's porosity, permeability, and fluid saturation.
10. Mineralogy: the types and relative amounts of minerals present in the rock. This property is important because it can affect the rock's physical and chemical properties, including its porosity, permeability, and ability to contain hydrocarbons.
11. Clay content: the percentage of the rock's volume that is made up of clay minerals. This property is important because clay can affect the rock's porosity, permeability, and ability to contain hydrocarbons.
12. Organic matter content: the percentage of the rock's volume that is made up of organic matter, such as kerogen. This property is important because it can indicate the potential for hydrocarbon generation and accumulation in the rock.
13. Acoustic impedance: the product of the rock's density and P-wave velocity. This property is important because it can be used to identify the presence of hydrocarbons in the rock.
14. Nuclear magnetic resonance (NMR) properties: the response of the rock's hydrogen atoms to magnetic fields. This property is important because it can be used to estimate the rock's porosity, permeability, and fluid saturation.
15. Capillary pressure: the pressure difference between the fluid in the rock's pore space and the fluid outside the rock. This property is important because it affects the ability of the fluid to flow through the rock.

These petrophysical properties are typically measured using a combination of laboratory techniques, including core analysis, well logging, and imaging. The results of petrophysical evaluations are used to create models of the subsurface reservoir, which can be used to predict the behavior of hydrocarbons and inform decisions about exploration, development, and production.

16. Mercury injection capillary pressure (MICP): the pressure required to force mercury into the pore space of the rock. This property is important because it can be used to determine the size distribution of the pores and estimate the rock's permeability.
17. X-ray diffraction (XRD): a technique used to identify the types of minerals present in the rock. This property is important because it can help to determine the rock's mineralogy and lithology.
18. Scanning electron microscopy (SEM): a technique used to image the rock at a microscopic level. This property is important because it can reveal details about the rock's structure, composition, and texture.
19. Fluid flow experiments: laboratory experiments that simulate the flow of fluids through the rock. This property is important because it can help to determine the rock's permeability and fluid flow properties.
20. Rock typing: the process of categorizing the rock into different types based on its petrophysical properties. This property is important because it can help to identify the most productive zones within the reservoir.
21. Resistivity imaging: a technique used to image the subsurface rock formations based on their electrical resistivity. This property is important because it can help to identify the presence of hydrocarbons and other fluids in the rock.
22. Magnetic resonance imaging (MRI): a technique used to image the subsurface rock formations based on their nuclear magnetic resonance properties. This property is important because it can provide information about the rock's porosity, permeability, and fluid saturation.
23. Rock mechanics testing: laboratory tests that measure the rock's strength, elasticity, and deformation behavior under various conditions. This property is important because it can help to determine the rock's stability and the potential for subsidence or other geomechanical issues during production.

Overall, the petrophysical evaluation of rock samples is a complex process that requires a variety of laboratory techniques and measurements. The resulting data is used to create models of the subsurface reservoir, which can be used to optimize the development and production of hydrocarbon resources.




Fluid inclusion Analysis and Microthermometry for solution of diagenetic problems

 



1. Fluid Inclusion Analysis


Across Earth's extensive history, the lithosphere has served as a reservoir for various fluids, whether they take the form of liquids, gases, or supercritical substances. These fluids have left an indelible mark by becoming encapsulated as minuscule, often microscopic inclusions within minerals. These inclusions predominantly encompass four distinct categories of fluids:

1. Aqueous solutions exhibiting a range of salinity levels.
2. Volatile elements, with CO2, CH4, and N2 as the primary constituents, found in varying proportions.
3. Hydrocarbons.
4. Aqueous solutions characterized by shifting salinity levels, potentially combined with volatile elements and/or hydrocarbons.

The scrutiny of these fluid inclusions serves as an invaluable source of insight into the physical and chemical properties of bygone fluids that once occupied diverse geological environments.

The primary analytical tool employed for this purpose is microthermometry, which hinges on the detection of temperature thresholds marking phase transitions within these inclusions. Fluid inclusion analysis finds extensive application across multiple disciplines, including the exploration and assessment of ore deposits, geothermal research, oil prospecting, as well as the study of metamorphic, magmatic, and sedimentary petrology. Moreover, it plays a pivotal role in unraveling the intricate relationships between fluid circulation and tectonic structures, among other research endeavors.

Fluid inclusions can be categorized based on the phases they contain at room temperature and the volumetric proportions between these phases. Here are the classifications:

A) A two-phase inclusion composed of both liquid and vapor, with a predominance of liquid.
B) A two-phase inclusion composed of both liquid and vapor, with a predominance of vapor.
C) A three-phase inclusion featuring two immiscible liquids (Liquid 1: aqueous solution, Liquid 2: CO2) and a gaseous phase (mostly consisting of CO2).
D) A three-phase inclusion containing liquid, vapor, and a solid (NaCl cube).



1.1 Methods


The cornerstone of all fluid inclusion research lies in microthermometric analyses.
Microthermometry involves the use of a heating/cooling stage integrated with an optical microscope.
This setup allows for the observation and recording of temperature changes occurring within fluid inclusions during controlled thermal cycles. By examining the recorded temperatures, it becomes possible to extract valuable insights into certain chemical and physical characteristics of the confined fluids.
These insights encompass parameters such as the salinity and molar volume of aqueous solutions, the presence of CO2 (and occasionally CH4 and/or N2) within the fluids, and the molar volume of fluid inclusions exclusively containing CO2, CH4, or N2. Additionally, when microthermometric data is combined with data acquired through micro-Raman spectroscopy, it enables the determination of the composition and molar volume of aqueous solutions containing volatile phases like CO2 and/or CH4 and/or N2.volume of aqueous solutions containing volatile phases (CO2 and/or CH4 and/or N2).
1.2 Application

The examination of fluid inclusions finds relevance across various disciplines within Earth sciences today, encompassing:

• The investigation of ore deposits, serving both the exploration of mining prospects and the understanding of ore formation.
• Geothermal energy research, contributing to the reconstruction of the development of geothermal systems and providing data for temperature assessments.
• Oil exploration
• The realms of sedimentary and metamorphic petrology.
• The field of structural geology, where it aids in the exploration of connections between fluid movement and tectonic structures.
• The domain of gemology, where it offers valuable insights and applications.
2. Microthermometry

Fluid inclusion microthermometry involves the meticulous quantification of both aqueous and petroleum fluid inclusions, utilizing a specialized temperature-controlled chamber that is seamlessly integrated with a petrographic microscope. This highly precise analytical technique allows for the comprehensive examination of phase changes and other critical phenomena occurring within individual fluid inclusions.
During the process, meticulous records are maintained of these observations.
These recorded observations are then meticulously compared with relevant phase diagrams or meticulously calibrated curves, resulting in the extraction of valuable data. This data encompasses crucial parameters such as temperature, salinity, and API gravity. The obtained temperature data can serve as a window into the history of petroleum emplacement, events related to cementation, or even the maximum thermal exposure experienced by the geological sample in question.
Furthermore, this analytical approach enables the assessment of proximity to the bubblepoint or dew point at the time of trapping, providing essential insights into the fluid's behavior under specific conditions.
The estimation of API gravity, with remarkable precision within a mere 2-degree range, is another valuable outcome of this meticulous analysis. Salinity measurements acquired through fluid inclusion microthermometry serve multiple purposes.
They offer clues regarding the origin of the fluids, shedding light on regional plumbing systems and their influence on the studied geological environment.
Additionally, salinity data plays a vital role in evaluating the composition of irreducible water within reservoirs. This information, in turn, facilitates precise calculations related to water saturation, a critical factor in reservoir characterization and resource assessment. In summary, fluid inclusion microthermometry is a sophisticated and invaluable analytical technique that allows for a deep exploration of the characteristics and histories of fluid inclusions.
It empowers geologists and researchers to unravel the secrets of geological processes, fluid behavior, and reservoir properties, contributing significantly to our understanding of the Earth's subsurface.

An oil and gas fluid inclusion in a sandstone thin section

Oil and gas fluid inclusion in sandstone thin section under UV light